Information card for entry 8102658

Structure parameters

• Chemical name: bis(1,10-phenanthroline)-fumarate-lead(II) nitrate, [Pb(C~12~H~8~N~2~)~2~(C~4~H~2~O~4~)~0.5~]~2~.2NO~3~
• Formula: C52 H34 N10 O10 Pb2
• Calculated formula: C52 H34 N10 O10 Pb2
• Title of publication: Crystal structure of tatrakis(1,10-phenanthroline)fumaratodilead(II) nitrate, [Pb2(C12H8N2)4(C4H2O4)](NO3)2
• Authors of publication: Yan-Ling Niu; Xiu-Mei Li; Qing-Wei Wang
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2010
• Journal volume: 225
• Journal issue: 1
• Pages of publication: 164
• a: 9.0544 ± 0.0019 Å
• b: 11.52 ± 0.002 Å
• c: 12.019 ± 0.003 Å
• α: 96.754 ± 0.003°
• β: 109.392 ± 0.002°
• γ: 100.347 ± 0.003°
• Cell volume: 1141.9 ± 0.4 ų
• Cell temperature: 292 ± 2 K
• Ambient diffraction temperature: 292 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0294
• Residual factor for significantly intense reflections: 0.027
• Weighted residual factors for significantly intense reflections: 0.0696
• Weighted residual factors for all reflections included in the refinement: 0.0708
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No