Information card for entry 8102868

Structure parameters

• Chemical name: bis(bis{2-[(2-isopropylaminoethylimino)methyl]- 5-methoxyphenolato}cobalt(III))tetrachlorocobalt(II), 2[Co(C~13~H~19~N~2~O~2~)~2~].[CoCl~4~]
• Formula: C52 H76 Cl4 Co3 N8 O8
• Calculated formula: C52 H76 Cl4 Co3 N8 O8
• Title of publication: Crystal structure of bis(bis{2-[(2-isopropylaminoethylimino)methyl]-5-methoxyphenolato}cobalt(III)) tetrachlorocobaltate(II), [Co(C13H19N2O2)2]2[CoCl4]
• Authors of publication: Ning Wang; Xiao-Yan Li
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2010
• Journal volume: 225
• Journal issue: 4
• Pages of publication: 803
• a: 26.206 ± 0.003 Å
• b: 16.655 ± 0.002 Å
• c: 17.081 ± 0.003 Å
• α: 90°
• β: 128.616 ± 0.002°
• γ: 90°
• Cell volume: 5825.1 ± 1.4 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0995
• Residual factor for significantly intense reflections: 0.0498
• Weighted residual factors for significantly intense reflections: 0.1161
• Weighted residual factors for all reflections included in the refinement: 0.1432
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No