Information card for entry 8102876

Structure parameters

• Chemical name: tetra-aqua-bis(dimethylformamide)-nickel(II) tetrachloroterephthalate, [Ni(C~3~H~7~NO)~2~(H~2~O)~4~](C~8~Cl~4~O~4~)
• Formula: C14 H22 Cl4 N2 Ni O10
• Calculated formula: C14 H22 Cl4 N2 Ni O10
• Title of publication: Crystal structure of tetraaquabis(dimethylformamide)nickel(II) tetrachloroterephthalate, [Ni(H2O)4(C3H7NO)2](C8Cl4O4)
• Authors of publication: Jiang-Quan Ma; Shou-Yong Xu
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2010
• Journal volume: 225
• Journal issue: 4
• Pages of publication: 791
• a: 5.736 ± 0.003 Å
• b: 8.536 ± 0.004 Å
• c: 12.027 ± 0.006 Å
• α: 95.874 ± 0.005°
• β: 101.998 ± 0.005°
• γ: 99.006 ± 0.005°
• Cell volume: 563.3 ± 0.5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0446
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for significantly intense reflections: 0.1335
• Weighted residual factors for all reflections included in the refinement: 0.1489
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No