Information card for entry 8103263

Structure parameters

• Formula: H104 Mo2 N6 O122 W24 Zn
• Calculated formula: H104.16 Mo2 N6 O122 W24 Zn
• Title of publication: Crystal structure of diammonium hexaaquazinc(II) bis[(?12-molybdato)-tetracosa(?2-oxo)-dodecaoxo-dodecatungsten] — ammonia — water (1:4:36), [NH4]2[Zn(H2O)6][(MoW12O40)2] • 4NH3 • 36H2O
• Authors of publication: Hai-Xing Liu
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2011
• Journal volume: 226
• Journal issue: 4
• Pages of publication: 441
• a: 22.54 ± 0.002 Å
• b: 22.54 ± 0.002 Å
• c: 22.54 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 11451.5 ± 1.8 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 225
• Hermann-Mauguin space group symbol: F m -3 m
• Hall space group symbol: -F 4 2 3
• Residual factor for all reflections: 0.0513
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for significantly intense reflections: 0.1147
• Weighted residual factors for all reflections included in the refinement: 0.1264
• Goodness-of-fit parameter for all reflections included in the refinement: 1.314
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No