Information card for entry 8103270

Structure parameters

• Formula: C31 H27.28 Cl Co N8 O6.14
• Calculated formula: C31.035 H27 Cl Co N8 O6.15
• Title of publication: Crystal structure of [tris(2-benzimidazolylmethyl)amine-N,N',N'',N'''](2-aminobenzoato-O)cobalt(II) perchlorate — water (1:0.14), [Co(C24H21N7)(C7H6NO2)][ClO4] · 0.14H2O
• Authors of publication: Jun-Yan Cui; Yong Hou; Feng-Mei Nie
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2012
• Journal volume: 227
• Journal issue: 1
• Pages of publication: 63
• a: 9.986 ± 0.004 Å
• b: 12.126 ± 0.005 Å
• c: 14.046 ± 0.005 Å
• α: 99.41 ± 0.003°
• β: 98.375 ± 0.004°
• γ: 111.299 ± 0.004°
• Cell volume: 1523.9 ± 1 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.053
• Residual factor for significantly intense reflections: 0.0392
• Weighted residual factors for significantly intense reflections: 0.1004
• Weighted residual factors for all reflections included in the refinement: 0.1056
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No