Information card for entry 8103296

Structure parameters

• Chemical name: catena-poly[[bis(benzo-15-crown-5)ammonium] [silver(I)-di-μ-sulfido-tungstate(VI)(Ag-W)-di-μ-sulfido]]
• Formula: C28 H40 Ag N O10 S4 W
• Calculated formula: C28 H40 Ag N O10 S4 W
• Title of publication: Crystal structure of catena-{[bis(benzo-15-crown-5)ammonium][silver(I)-tetrakis(m-sulfido)tungstate(VI)], [(C14H20O5)2(NH4)][AgWS4]
• Authors of publication: Yuan Cao; Guosheng Cheng; Guozhu Shen
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2012
• Journal volume: 227
• Journal issue: 1
• Pages of publication: 50
• a: 12.915 ± 0.003 Å
• b: 11.515 ± 0.002 Å
• c: 24.758 ± 0.005 Å
• α: 90°
• β: 92.12 ± 0.03°
• γ: 90°
• Cell volume: 3679.4 ± 1.3 ų
• Cell temperature: 291 ± 2 K
• Ambient diffraction temperature: 291 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0742
• Residual factor for significantly intense reflections: 0.059
• Weighted residual factors for significantly intense reflections: 0.1518
• Weighted residual factors for all reflections included in the refinement: 0.1642
• Goodness-of-fit parameter for all reflections included in the refinement: 0.983
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No