Information card for entry 8104565

Structure parameters

• Formula: C27 H29 N3 O8 Pb
• Calculated formula: C27 H29 N3 O8 Pb
• Title of publication: Crystal structure of diaqua-bis(μ2-6-phenylpyridine-2-carboxylate-κ3N,O:O)-bis(6-phenylpyridine-2-carboxylato-κ2N,O)lead(II) – N,N-dimethylformamide – water (1/2/4), C54H58N6O16Pb2
• Authors of publication: Tai, Xi-Shi; Liang, Lei; Li, Xiang-Tao; Cao, Shu-Hua; Wang, Li-Hua
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2021
• Journal volume: 236
• Journal issue: 6
• Pages of publication: 1199 - 1201
• a: 9.469 ± 0.0006 Å
• b: 12.9374 ± 0.0006 Å
• c: 13.2303 ± 0.0007 Å
• α: 63.395 ± 0.005°
• β: 74.291 ± 0.005°
• γ: 69.113 ± 0.005°
• Cell volume: 1341.9 ± 0.14 ų
• Cell temperature: 149.99 ± 0.1 K
• Ambient diffraction temperature: 149.99 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0333
• Residual factor for significantly intense reflections: 0.0284
• Weighted residual factors for significantly intense reflections: 0.0464
• Weighted residual factors for all reflections included in the refinement: 0.0484
• Goodness-of-fit parameter for all reflections included in the refinement: 0.99
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No