Information card for entry 8104717

Structure parameters

• Formula: C32 H54 Li2 N4 Si2
• Calculated formula: C32 H54 Li2 N4 Si2
• Title of publication: The crystal structure of bis{(μ2-3,3-dimethyl-1-phenylbut-1-en-2-yl)((dimethylamino)dimethylsilyl)amido-κ3 N,N′:N′}dilithium, C32H54Li2N4Si2
• Authors of publication: Tong, Hong-Bo; Wang, Meng-Liang
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2021
• Journal volume: 236
• Journal issue: 4
• Pages of publication: 803 - 805
• a: 11.611 ± 0.004 Å
• b: 11.157 ± 0.006 Å
• c: 13.307 ± 0.005 Å
• α: 90°
• β: 100.12 ± 0.03°
• γ: 90°
• Cell volume: 1697 ± 1.3 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.065
• Residual factor for significantly intense reflections: 0.0622
• Weighted residual factors for significantly intense reflections: 0.1539
• Weighted residual factors for all reflections included in the refinement: 0.1561
• Goodness-of-fit parameter for all reflections included in the refinement: 1.008
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No