Information card for entry 8105088

Structure parameters

• Formula: C20 H30 N4 O4 P2 S4 Zn
• Calculated formula: C20 H30 N4 O4 P2 S4 Zn
• Title of publication: Crystal structure of catena-[(bis(O,O′-diethyl dithiophosphato-S,S′)-μ2-1,2-bis(3-pyridylmethylene)hydrazine-N,N′)zinc(II)], {C20H30N4O4P2S4Zn}n
• Authors of publication: Tan, Yee Seng; Tiekink, Edward R.T.
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2020
• Journal volume: 235
• Journal issue: 2
• Pages of publication: 297 - 299
• a: 8.0184 ± 0.0001 Å
• b: 8.4326 ± 0.0001 Å
• c: 23.5086 ± 0.0002 Å
• α: 80.478 ± 0.001°
• β: 80.679 ± 0.001°
• γ: 76.112 ± 0.001°
• Cell volume: 1509.37 ± 0.03 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0475
• Residual factor for significantly intense reflections: 0.0449
• Weighted residual factors for significantly intense reflections: 0.1158
• Weighted residual factors for all reflections included in the refinement: 0.1182
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No