Information card for entry 8105104

Structure parameters

• Chemical name: dichloro[1,1-di-<i>p</i>-tolyl-<i>N</i>-(2-methylbenzene) phosphinamide-<i>k</i>P](methyl-di-<i>p</i>- tolylphosphinite-<i>k</i>P)-palladium(II)
• Formula: C36 H39 Cl2 N O P2 Pd
• Calculated formula: C36 H39 Cl2 N O P2 Pd
• Title of publication: Crystal structure of dichlorido(N-o-tolyl-1,1-di-p-tolylphosphanamine–κ1 P)-(methoxydi-p-tolylphosphane-κ1 P)palladium(II), C36H39Cl2NOP2Pd
• Authors of publication: Kama, Dumisani V.; Brink, Alice; Roodt, Andreas
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2020
• Journal volume: 235
• Journal issue: 2
• Pages of publication: 349 - 352
• a: 19.209 ± 0.013 Å
• b: 15.144 ± 0.011 Å
• c: 24.011 ± 0.019 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6985 ± 9 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0491
• Residual factor for significantly intense reflections: 0.0292
• Weighted residual factors for significantly intense reflections: 0.0706
• Weighted residual factors for all reflections included in the refinement: 0.0867
• Goodness-of-fit parameter for all reflections included in the refinement: 1.127
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No