Information card for entry 8105228

Structure parameters

• Formula: C26 H20 N2 O7 Pb
• Calculated formula: C26 H20 N2 O7 Pb
• Title of publication: Crystal structure of bis[(μ2-4⋯O,O′:O′)-(4-hydroxybenzoato-κ2 O,O′)-(1,10-phenanthroline-κ2 N,N′)]-di-lead(II)μ-4-hydroxybenzoato-κ3 O,O′:O′;κ3 O,O′:O′-bis-[(4-hydroxybenzoato-κ2 O,O′)bis(1,10-phenanthroline-κ2 N,N′)di-lead(II)] monohydrate, C52H36N4O12Pb2 ⋅ H2O
• Authors of publication: Dai, Ben-Cai; Liu, Chang-Chun; Zhou, Yang; Chen, Jin; Fu, Yang; Zhao, Pei-Zheng
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2020
• Journal volume: 235
• Journal issue: 3
• Pages of publication: 589 - 591
• a: 13.7767 ± 0.0001 Å
• b: 7.9925 ± 0.0001 Å
• c: 21.249 ± 0.0002 Å
• α: 90°
• β: 93.149 ± 0.001°
• γ: 90°
• Cell volume: 2336.2 ± 0.04 ų
• Cell temperature: 169.99 ± 0.1 K
• Ambient diffraction temperature: 169.99 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.023
• Residual factor for significantly intense reflections: 0.022
• Weighted residual factors for significantly intense reflections: 0.0574
• Weighted residual factors for all reflections included in the refinement: 0.0582
• Goodness-of-fit parameter for all reflections included in the refinement: 1.074
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No