Information card for entry 8105278

Structure parameters

• Formula: C68 H100 Cl8 P2 Pd
• Calculated formula: C68 H100 Cl8 P2 Pd
• Title of publication: The crystal structure of dichlorobis(2-(dicyclohexylphosphino)-2′,4′,6′-tri-i-propyl-1,1′-biphenyl) palladium(II)-dichloroform, C68H100Cl8P2Pd
• Authors of publication: Liu, Hui
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2020
• Journal volume: 235
• Journal issue: 3
• Pages of publication: 755 - 757
• a: 9.6961 ± 0.0004 Å
• b: 13.6096 ± 0.0006 Å
• c: 15.1642 ± 0.0005 Å
• α: 88.456 ± 0.003°
• β: 72.251 ± 0.003°
• γ: 72.376 ± 0.004°
• Cell volume: 1811.65 ± 0.14 ų
• Cell temperature: 291 ± 2 K
• Ambient diffraction temperature: 291.15 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0554
• Residual factor for significantly intense reflections: 0.0483
• Weighted residual factors for significantly intense reflections: 0.126
• Weighted residual factors for all reflections included in the refinement: 0.1332
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No