Information card for entry 8105295

Structure parameters

• Formula: C44 H56 N10 Ni O6 S2
• Calculated formula: C44 H56 N10 Ni O6 S2
• Title of publication: Crystal structure of bis(N,2-bis(4-ethoxybenzylidene)hydrazine-1-carbohydrazonothioato-κ2 N,S)nickel(II) — N,N-dimethylformamide (1/2), C44H56N10S2O6Ni
• Authors of publication: Li, Zhuang-Yu; Liu, E.; Liu, Xiao-Jing; Jian, Fang-Fang; Liang, Tong-ling
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2020
• Journal volume: 235
• Journal issue: 4
• Pages of publication: 811 - 813
• a: 9.3077 ± 0.0014 Å
• b: 9.9624 ± 0.0014 Å
• c: 14.0449 ± 0.0019 Å
• α: 70.889 ± 0.003°
• β: 75.532 ± 0.002°
• γ: 87.544 ± 0.003°
• Cell volume: 1190.5 ± 0.3 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1053
• Residual factor for significantly intense reflections: 0.0528
• Weighted residual factors for significantly intense reflections: 0.1037
• Weighted residual factors for all reflections included in the refinement: 0.1279
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No