Information card for entry 8105478

Structure parameters

• Formula: C31 H29 Cl2 F6 N3 P Rh
• Calculated formula: C31 H29 Cl2 F6 N3 P Rh
• Title of publication: Crystal structure of chlorido-(η 5-pentamethylcyclopentadienyl)-(4-chloro-4-pyridyl-2,2′:6′,2′′-terpyridine-κ2N,N′) rhodium(III) hexaflourophosphate, C31H29Cl2F6N3PRh
• Authors of publication: Gichumbi, Joel M.; Zamisa, Sizwe J.; Friedrich, Holger B.
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2020
• Journal volume: 235
• Journal issue: 6
• Pages of publication: 1403 - 1405
• a: 7.4069 ± 0.0007 Å
• b: 13.2451 ± 0.0012 Å
• c: 32.141 ± 0.003 Å
• α: 90°
• β: 93.924 ± 0.002°
• γ: 90°
• Cell volume: 3145.8 ± 0.5 ų
• Cell temperature: 123.15 K
• Ambient diffraction temperature: 123.15 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.053
• Residual factor for significantly intense reflections: 0.0386
• Weighted residual factors for significantly intense reflections: 0.089
• Weighted residual factors for all reflections included in the refinement: 0.0962
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No