Information card for entry 8105482

Structure parameters

• Formula: C44 H54 N10 O7 Pb
• Calculated formula: C44 H54 N10 O7 Pb
• Title of publication: The crystal structure of aqua{N,N,N′,N′-tetrakis[(1H-benzimidazol-κN 3) methyl]cyclohexane-1,2-diamine}lead(II) diacetate–methanol (1/2), C44H54N10O7Pb
• Authors of publication: Li, Ji; Miao, Ming-Zhi
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2020
• Journal volume: 235
• Journal issue: 6
• Pages of publication: 1417 - 1420
• a: 12.096 ± 0.002 Å
• b: 12.916 ± 0.0002 Å
• c: 16.5904 ± 0.0007 Å
• α: 101.163 ± 0.002°
• β: 110.634 ± 0.002°
• γ: 100.698 ± 0.002°
• Cell volume: 2287 ± 0.4 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0691
• Residual factor for significantly intense reflections: 0.0604
• Weighted residual factors for significantly intense reflections: 0.1352
• Weighted residual factors for all reflections included in the refinement: 0.1409
• Goodness-of-fit parameter for all reflections included in the refinement: 1.091
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No