Information card for entry 8105576

Structure parameters

• Chemical name: (1,4,10,13-Tetraoxa-7,16-diazacyclooctadecane-κ^6^N~2~,O~4~) rubidium 1,2,3,4,5-pentamethyl-cyclopentadienide
• Formula: C22 H41 N2 O4 Rb
• Calculated formula: C22 H41 N2 O4 Rb
• Title of publication: Crystal structure of [(1,2-η)-1,2,3,4,5-pentamethyl-cyclopenta-2,4-dien-1-yl] (1,4,10,13-tetraoxa-7,16-diazacyclooctadecane-κ6 N 2,O 4) rubidium (I), [Rb(diaza-18-crown-6)]Cp*, C22H41N2O4Rb
• Authors of publication: Henneberger, Thomas; Klein, Wilhelm; Fässler, Thomas F.
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2018
• Journal volume: 234
• Journal issue: 1
• Pages of publication: 165 - 167
• a: 10.816 ± 0.0009 Å
• b: 17.7253 ± 0.0016 Å
• c: 13.2179 ± 0.0012 Å
• α: 90°
• β: 93.961 ± 0.008°
• γ: 90°
• Cell volume: 2528 ± 0.4 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1009
• Residual factor for significantly intense reflections: 0.0376
• Weighted residual factors for significantly intense reflections: 0.062
• Weighted residual factors for all reflections included in the refinement: 0.0694
• Goodness-of-fit parameter for all reflections included in the refinement: 0.718
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No