Information card for entry 8105864

Structure parameters

• Formula: C36 H66 N4 O8 P4 S8 Zn2
• Calculated formula: C36 H66 N4 O8 P4 S8 Zn2
• Title of publication: Crystal structure of tetrakis(O,O′-diisopropyldithiophosphato-κ2 S,S′)-(μ2-1,2-bis(4-pyridylmethylene)hydrazine-κ2 N:N′)zinc(II), C36H66N4O8P4S8Zn2
• Authors of publication: Tan, Yee Seng; Tiekink, Edward R.T.
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2019
• Journal volume: 234
• Journal issue: 4
• Pages of publication: 827 - 829
• a: 7.9496 ± 0.0001 Å
• b: 11.5638 ± 0.0002 Å
• c: 16.5616 ± 0.0002 Å
• α: 75.604 ± 0.001°
• β: 86.321 ± 0.001°
• γ: 83.103 ± 0.002°
• Cell volume: 1463.06 ± 0.04 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.045
• Residual factor for significantly intense reflections: 0.0424
• Weighted residual factors for significantly intense reflections: 0.1057
• Weighted residual factors for all reflections included in the refinement: 0.1072
• Goodness-of-fit parameter for all reflections included in the refinement: 1.176
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No