Information card for entry 8106040

Structure parameters

• Formula: C52 H40 N2 O9 Pb
• Calculated formula: C52 H40 N2 O9 Pb
• Title of publication: Crystal structure of 4-(4′-(pyridin-4-yl)-[1,1′-biphenyl]-4-yl)pyridin-1-ium catena-poly[{5-carboxy-4′-methyl-[1,1′-biphenyl]-3-carboxylato-κ2 O,O′}-(μ2-4′-methyl-[1,1′-biphenyl]-3,5-dicarboxylato-κ4 O,O′:O′′,O′′′)lead(II)], C52H40N2O9Pb
• Authors of publication: Song, Wei; Li, Shi-Hui; Xu, Xue-Li
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2018
• Journal volume: 233
• Journal issue: 1
• Pages of publication: 51 - 53
• a: 10.3025 ± 0.0004 Å
• b: 14.174 ± 0.0009 Å
• c: 16.0428 ± 0.0009 Å
• α: 115.835 ± 0.006°
• β: 97.68 ± 0.004°
• γ: 90.493 ± 0.004°
• Cell volume: 2083.8 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0395
• Residual factor for significantly intense reflections: 0.0342
• Weighted residual factors for significantly intense reflections: 0.0578
• Weighted residual factors for all reflections included in the refinement: 0.0612
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No