Information card for entry 8106100

Structure parameters

• Formula: C14 H38 B10 Br2 Ni P2
• Calculated formula: C14 H38 B10 Br2 Ni P2
• Title of publication: Crystal structure of dibromido[(1,2-bis(diisopropylphosphino)-1,2-dicarba-closo-dodecaborane-κ2 P,P′]nickel(II), C14H38B10NiBr2P2
• Authors of publication: Liguo, Yang; Qingyun, Liu; Xin, Wang; Qianqian, Gao; Yuqiang, Dai
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2018
• Journal volume: 233
• Journal issue: 2
• Pages of publication: 205 - 207
• a: 10.192 ± 0.0014 Å
• b: 19.055 ± 0.002 Å
• c: 13.5243 ± 0.0017 Å
• α: 90°
• β: 103.394 ± 0.002°
• γ: 90°
• Cell volume: 2555.1 ± 0.5 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1048
• Residual factor for significantly intense reflections: 0.0461
• Weighted residual factors for significantly intense reflections: 0.0728
• Weighted residual factors for all reflections included in the refinement: 0.0869
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No