Information card for entry 8106379

Structure parameters

• Formula: C30 H30 Cu Ge N8 O41 W12
• Calculated formula: C30 H30 Cu Ge N8 O41 W12
• Title of publication: Crystal structure of catena-poly[bis(4,4′-dipyridylaminium-kN)-(μ2-germanowolframato-κ2 O:O′)-(2,2′-bipyridine-κ2 N,N′)copper(II)] with a Keggin-type heteropolyoxoanion, [Cu(C10H8N2)(C10H10N3)2][GeW12O40] ⋅ H2O
• Authors of publication: Wu, Li-Zhou
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2018
• Journal volume: 233
• Journal issue: 6
• Pages of publication: 1007 - 1010
• a: 12.095 ± 0.002 Å
• b: 13.488 ± 0.003 Å
• c: 19.22 ± 0.004 Å
• α: 90.221 ± 0.003°
• β: 92.188 ± 0.003°
• γ: 108.966 ± 0.003°
• Cell volume: 2962.7 ± 1 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296.15 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0822
• Residual factor for significantly intense reflections: 0.0624
• Weighted residual factors for significantly intense reflections: 0.1497
• Weighted residual factors for all reflections included in the refinement: 0.1622
• Goodness-of-fit parameter for all reflections included in the refinement: 0.988
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No