Information card for entry 8106439

Structure parameters

• Formula: C54 H64 Ag2 B20 Cl4 N2 O6 P4
• Calculated formula: C54 H64 Ag2 B20 Cl4 N2 O6 P4
• Title of publication: Crystal structure of bis(μ-nitrato-κ2 O:O)-bis[1,2-bis(diphenylphosphino)-1,2-dicarba-closo-dodecaborane-κ2 P,P′]disilver(I) dicloromethane monosolvate, C54H64B20Cl4O6P4Ag2
• Authors of publication: Yanfei, Wang; Xin, Wang; Qianqian, Gao; Liguo, Yang
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2017
• Journal volume: 232
• Journal issue: 1
• Pages of publication: 81 - 83
• a: 10.12 ± 0.001 Å
• b: 11.9101 ± 0.0011 Å
• c: 14.4999 ± 0.0015 Å
• α: 86.432 ± 0.002°
• β: 80.67 ± 0.001°
• γ: 84.031 ± 0.002°
• Cell volume: 1713.4 ± 0.3 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0738
• Residual factor for significantly intense reflections: 0.0535
• Weighted residual factors for significantly intense reflections: 0.14
• Weighted residual factors for all reflections included in the refinement: 0.1544
• Goodness-of-fit parameter for all reflections included in the refinement: 0.981
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No