Information card for entry 8106990

Structure parameters

• Formula: C20 H15.5 Cl N1.5 Pd0.5
• Calculated formula: C40 H31 Cl2 N3 Pd
• Title of publication: Crystal structure of trans-dichlorido[1,3-bis(9-methyl-9H-fluoren-9-yl) benzimidazol-2-ylidene](pyridine)palladium(II) – a compound with anagostic CH–Pd interactions, C40H31Cl2N3Pd
• Authors of publication: Teci, Matthieu; Brenner, Eric; Matt, Dominique; Toupet, Loïc
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2016
• Journal volume: 231
• Journal issue: 3
• Pages of publication: 733 - 735
• a: 16.7821 ± 0.0007 Å
• b: 17.1436 ± 0.0008 Å
• c: 11.1431 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3205.9 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0834
• Residual factor for significantly intense reflections: 0.0394
• Weighted residual factors for significantly intense reflections: 0.0752
• Weighted residual factors for all reflections included in the refinement: 0.0817
• Goodness-of-fit parameter for all reflections included in the refinement: 0.837
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No