Information card for entry 8107106

Structure parameters

• Formula: C56 H58 Cl2 O4 P4 Pd2
• Calculated formula: C56 H58 Cl2 O4 P4 Pd2
• Title of publication: Crystal structure of bis(μ 2-chlorido)-bis(di-p-tolylhydroxyphosphine-κP)-bis(di-p-tolylphosphite-κP)dipalladium(II), C56H58Cl2O4P4Pd2
• Authors of publication: Kama, Dumisani V.; Brink, Alice; Visser, Hendrik G.
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2016
• Journal volume: 231
• Journal issue: 4
• Pages of publication: 1081 - 1083
• a: 12.736 ± 0.002 Å
• b: 18.187 ± 0.002 Å
• c: 12.335 ± 0.002 Å
• α: 90°
• β: 109.053 ± 0.004°
• γ: 90°
• Cell volume: 2700.6 ± 0.7 ų
• Cell temperature: 101 ± 2 K
• Ambient diffraction temperature: 101 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0396
• Residual factor for significantly intense reflections: 0.034
• Weighted residual factors for all reflections included in the refinement: 0.0955
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No