Information card for entry 8107474

Structure parameters

• Formula: C68 H54 N4 O9 Pb2
• Calculated formula: C68 H54 N4 O9 Pb2
• Title of publication: The crystal structure of di-μ-1-naphthylacetato-κ 3 O,O′:O;κ 3 O:O,O′-bis[(1-naphthylacetato-κ 2 O,O′)(2,2′-bipyridine-κ 2 N,N′)lead(II)] monohydrate, C68H54N4O9Pb2
• Authors of publication: Deng, Zheyu; Li, Jiahong; Hou, Xinbo; Luo, Na; Zhu, Xiaoming
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2023
• Journal volume: 238
• Journal issue: 3
• Pages of publication: 483 - 485
• a: 15.7286 ± 0.0014 Å
• b: 16.3623 ± 0.0014 Å
• c: 22.5 ± 0.002 Å
• α: 90°
• β: 97.369 ± 0.001°
• γ: 90°
• Cell volume: 5742.7 ± 0.9 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0258
• Residual factor for significantly intense reflections: 0.0203
• Weighted residual factors for significantly intense reflections: 0.0474
• Weighted residual factors for all reflections included in the refinement: 0.0488
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No