Information card for entry 1549759

Structure parameters

• Formula: C21 H18 Al F28 Li O12
• Calculated formula: C21 H18 Al F28 Li O12
• Title of publication: Facile and systematic access to the least-coordinating WCA [(R^FO)₃Al-F-Al(OR^F)₃]^- and its more Lewis-basic brother [F-Al(OR^F)₃]^- (R^F = C(CF₃)₃).
• Authors of publication: Martens, Arthur; Weis, Philippe; Krummer, Michael Christian; Kreuzer, Marvin; Meierhöfer, Andreas; Meier, Stefan C.; Bohnenberger, Jan; Scherer, Harald; Riddlestone, Ian; Krossing, Ingo
• Journal of publication: Chemical science
• Year of publication: 2018
• Journal volume: 9
• Journal issue: 35
• Pages of publication: 7058 - 7068
• a: 35.9221 ± 0.0016 Å
• b: 10.7468 ± 0.0005 Å
• c: 19.3985 ± 0.0009 Å
• α: 90°
• β: 102.381 ± 0.002°
• γ: 90°
• Cell volume: 7314.6 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0618
• Residual factor for significantly intense reflections: 0.0449
• Weighted residual factors for significantly intense reflections: 0.1036
• Weighted residual factors for all reflections included in the refinement: 0.1132
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No