Crystallography Open Database

Information card for entry 1559719

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Coordinates	1559719.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37.5 H54 N2 Si Zn
Calculated formula	C37.5 H54 N2 Si Zn
Title of publication	A cyclopentadienyl functionalized silylene ‒ a flexible ligand for Si- and C-coordination
Authors of publication	Kaufmann, Sebastian; Krätschmer, Frederic; Köppe, Ralf; Schon, Thorben; Schoo, Christoph; Roesky, Peter W.
Journal of publication	Chemical Science
Year of publication	2020
Journal volume	11
Journal issue	46
Pages of publication	12446 - 12452
a	11.4292 ± 0.0005 Å
b	20.8212 ± 0.0011 Å
c	16.8791 ± 0.0007 Å
α	90°
β	97.269 ± 0.003°
γ	90°
Cell volume	3984.4 ± 0.3 Å³
Cell temperature	210 K
Ambient diffraction temperature	210 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1027
Residual factor for significantly intense reflections	0.0577
Weighted residual factors for significantly intense reflections	0.151
Weighted residual factors for all reflections included in the refinement	0.1689
Goodness-of-fit parameter for all reflections included in the refinement	0.954
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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