Crystallography Open Database

Information card for entry 1559720

Preview

Coordinates	1559720.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H54 N2 Si Zn
Calculated formula	C36 H54 N2 Si Zn
Title of publication	A cyclopentadienyl functionalized silylene ‒ a flexible ligand for Si- and C-coordination
Authors of publication	Kaufmann, Sebastian; Krätschmer, Frederic; Köppe, Ralf; Schon, Thorben; Schoo, Christoph; Roesky, Peter W.
Journal of publication	Chemical Science
Year of publication	2020
Journal volume	11
Journal issue	46
Pages of publication	12446 - 12452
a	8.5961 ± 0.0004 Å
b	10.5095 ± 0.0003 Å
c	19.1188 ± 0.0009 Å
α	90°
β	99.139 ± 0.004°
γ	90°
Cell volume	1705.28 ± 0.12 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	5
Space group number	7
Hermann-Mauguin space group symbol	P 1 c 1
Hall space group symbol	P -2yc
Residual factor for all reflections	0.0345
Residual factor for significantly intense reflections	0.0293
Weighted residual factors for significantly intense reflections	0.0659
Weighted residual factors for all reflections included in the refinement	0.0671
Goodness-of-fit parameter for all reflections included in the refinement	0.986
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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