Crystallography Open Database

Information card for entry 1574672

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Coordinates	1574672.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H72 B10 Bi N4 Si2
Calculated formula	C32 H56 B10 Bi N4 Si2
Title of publication	Isolable monoatomic monovalent bismuth complexes with a redox non-innocent bis-silylenyl carborane ligand
Authors of publication	Xu, Jian; Yao, Shenglai; Postils, Verònica; Matito, Eduard; Lorent, Christian; Driess, Matthias
Journal of publication	Chemical Science
Year of publication	2025
Journal volume	16
Journal issue	24
Pages of publication	10826 - 10832
a	23.2329 ± 0.0004 Å
b	18.601 ± 0.0004 Å
c	13.6308 ± 0.0003 Å
α	90°
β	90°
γ	90°
Cell volume	5890.6 ± 0.2 Å³
Cell temperature	110.07 ± 0.12 K
Ambient diffraction temperature	111.15 K
Number of distinct elements	6
Space group number	63
Hermann-Mauguin space group symbol	C m c m
Hall space group symbol	-C 2c 2
Residual factor for all reflections	0.0611
Residual factor for significantly intense reflections	0.0561
Weighted residual factors for significantly intense reflections	0.1501
Weighted residual factors for all reflections included in the refinement	0.1545
Goodness-of-fit parameter for all reflections included in the refinement	1.096
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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