Information card for entry 1575460

Structure parameters

• Formula: C16 H136 B6 Ge4 N8 Na2 Ni24 O206 W41.34
• Calculated formula: C16 H72 B6 Ge4 N8 Na2 Ni24 O206 W41.334
• Title of publication: A tetrameric polyoxometalate with two orderly and dense double-layered {Ni₁₂W_8/3} cluster centers.
• Authors of publication: Lian, Chen; Yang, Guo-Yu
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2025
• Journal volume: 61
• Journal issue: 75
• Pages of publication: 14402 - 14405
• a: 14.6148 ± 0.0005 Å
• b: 18.4469 ± 0.0009 Å
• c: 24.2042 ± 0.001 Å
• α: 112.296 ± 0.004°
• β: 93.446 ± 0.003°
• γ: 105.01 ± 0.003°
• Cell volume: 5739.2 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.107
• Residual factor for significantly intense reflections: 0.0604
• Weighted residual factors for significantly intense reflections: 0.1639
• Weighted residual factors for all reflections included in the refinement: 0.2248
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No