Information card for entry 1577009

Structure parameters

• Formula: C54 H43 Cl N2 Pd
• Calculated formula: C54 H43 Cl N2 Pd
• Title of publication: Achieving (quasi)-monocoordination in metal complexes with an exceptionally bulky carbene ligand.
• Authors of publication: Zapf, Ludwig; Rivard, Eric
• Journal of publication: Chemical science
• Year of publication: 2026
• Journal volume: 17
• Journal issue: 13
• Pages of publication: 6500 - 6506
• a: 10.1901 ± 0.0004 Å
• b: 21.5445 ± 0.0011 Å
• c: 35.5333 ± 0.0018 Å
• α: 90°
• β: 93.017 ± 0.002°
• γ: 90°
• Cell volume: 7790.2 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0373
• Residual factor for significantly intense reflections: 0.0317
• Weighted residual factors for significantly intense reflections: 0.0732
• Weighted residual factors for all reflections included in the refinement: 0.0785
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Diffraction radiation X-ray symbol: K-L~2,3~
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No