Reactions between arylhydrazinium chlorides and 2-chloroquinoline-3-carbaldehydes: molecular and supramolecular structures of a hydrazone, a 4,9-dihydro-1<i>H</i>-pyrazolo[3,4-<i>b</i>]quinoline and two 1<i>H</i>-pyrazolo[3,4-<i>b</i>]quinolines
Authors of publication
Kumara, Tholappanavara H. Suresha; Nagendrappa, Gopalpur; Chandrika, Nanjappa; Sowmya, Haliwana B. V.; Kaur, Manpreet; Jasinski, Jerry P.; Glidewell, Christopher
Journal of publication
Acta Crystallographica Section C
Year of publication
2016
Journal volume
72
Journal issue
9
a
25.145 ± 0.002 Å
b
16.9623 ± 0.0019 Å
c
16.8138 ± 0.0019 Å
α
90°
β
90°
γ
90°
Cell volume
7171.4 ± 1.3 Å3
Cell temperature
300 ± 2 K
Ambient diffraction temperature
300 ± 2 K
Number of distinct elements
3
Space group number
60
Hermann-Mauguin space group symbol
P b c n
Hall space group symbol
-P 2n 2ab
Residual factor for all reflections
0.0821
Residual factor for significantly intense reflections
0.0471
Weighted residual factors for significantly intense reflections
0.1002
Weighted residual factors for all reflections included in the refinement
0.1187
Goodness-of-fit parameter for all reflections included in the refinement
