Reactions between arylhydrazinium chlorides and 2-chloroquinoline-3-carbaldehydes: molecular and supramolecular structures of a hydrazone, a 4,9-dihydro-1<i>H</i>-pyrazolo[3,4-<i>b</i>]quinoline and two 1<i>H</i>-pyrazolo[3,4-<i>b</i>]quinolines
Authors of publication
Kumara, Tholappanavara H. Suresha; Nagendrappa, Gopalpur; Chandrika, Nanjappa; Sowmya, Haliwana B. V.; Kaur, Manpreet; Jasinski, Jerry P.; Glidewell, Christopher
Journal of publication
Acta Crystallographica Section C
Year of publication
2016
Journal volume
72
Journal issue
9
a
29.9202 ± 0.0012 Å
b
29.9202 ± 0.0012 Å
c
7.3811 ± 0.0003 Å
α
90°
β
90°
γ
120°
Cell volume
5722.4 ± 0.4 Å3
Cell temperature
296 ± 2 K
Ambient diffraction temperature
296 ± 2 K
Number of distinct elements
3
Space group number
148
Hermann-Mauguin space group symbol
R -3 :H
Hall space group symbol
-R 3
Residual factor for all reflections
0.0814
Residual factor for significantly intense reflections
0.0564
Weighted residual factors for significantly intense reflections
0.1468
Weighted residual factors for all reflections included in the refinement
0.1729
Goodness-of-fit parameter for all reflections included in the refinement
