Information card for entry 2203070

Structure parameters

• Formula: C46 H51 B F24 N2 Si2
• Calculated formula: C46 H51 B F24 N2 Si2
• Title of publication: Dimethyl(2-trimethylsilylethyl)[(2-trimethylsilylethyl)dimethylammonio]ammonium tetrakis[3,5-bis(trifluoromethyl)phenyl]borate at 130K
• Authors of publication: Kathryn Hassall; Jonathan White
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2004
• Journal volume: 60
• Journal issue: 1
• Pages of publication: o107 - o108
• a: 17.1047 ± 0.0011 Å
• b: 16.8652 ± 0.0011 Å
• c: 18.9828 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5476 ± 0.6 ų
• Cell temperature: 130 ± 0.2 K
• Ambient diffraction temperature: 130 ± 0.2 K
• Number of distinct elements: 6
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.0577
• Residual factor for significantly intense reflections: 0.0464
• Weighted residual factors for significantly intense reflections: 0.1196
• Weighted residual factors for all reflections included in the refinement: 0.1261
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No