Information card for entry 2219751

Structure parameters

• Chemical name: [2,6-Bis(di-<i>tert</i>-butylphosphinomethyl)phenyl- κ^3^<i>P</i>,<i>C</i>^1^,<i>P</i>'](nitrato-κ<i>O</i>)nickel(II)
• Formula: C24 H43 N Ni O3 P2
• Calculated formula: C24 H43 N Ni O3 P2
• Title of publication: [2,6-Bis(di-<i>tert</i>-butylphosphinomethyl)phenyl-κ^3^<i>P</i>,<i>C</i>^1^,<i>P</i>'](nitrato-κ<i>O</i>)nickel(II)
• Authors of publication: Boro, Brian J.; Dickie, Diane A.; Duesler, Eileen N.; Goldberg, Karen I.; Kemp, Richard A.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 11
• Pages of publication: m1402
• a: 24.0023 ± 0.0014 Å
• b: 12.635 ± 0.0006 Å
• c: 17.6528 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5353.5 ± 0.4 ų
• Cell temperature: 225 ± 2 K
• Ambient diffraction temperature: 225 ± 2 K
• Number of distinct elements: 6
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.035
• Residual factor for significantly intense reflections: 0.0301
• Weighted residual factors for significantly intense reflections: 0.093
• Weighted residual factors for all reflections included in the refinement: 0.0988
• Goodness-of-fit parameter for all reflections included in the refinement: 0.805
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes