Information card for entry 2232760

Structure parameters

• Chemical name: <i>catena</i>-Poly[[[bis(methanol-κ<i>O</i>)lead(II)]-μ- <i>N</i>'-[1-(pyridin-2-yl-κ<i>N</i>)ethylidene]isonicotinohydrazidato- κ^3^<i>N</i>',<i>O</i>:<i>N</i>^1^] perchlorate]
• Formula: C15 H19 Cl N4 O7 Pb
• Calculated formula: C15 H19 Cl N4 O7 Pb
• SMILES: [Pb]12(OC(=N[N]2=C(c2[n]1cccc2)C)c1ccncc1)([OH]C)[n]1ccc(C2O[Pb]3([OH]C)[n]4c(cccc4)C(=[N]3N=2)C)cc1.Cl(=O)(=O)(=O)[O-].OC.Cl(=O)(=O)(=O)[O-].OC
• Title of publication: <i>catena</i>-Poly[[[bis(methanol-κ<i>O</i>)lead(II)]-μ-<i>N</i>'-[1-(pyridin-2-yl-κ<i>N</i>)ethylidene]isonicotinohydrazidato-κ^3^<i>N</i>',<i>O</i>:<i>N</i>^1^] perchlorate]
• Authors of publication: Shahverdizadeh, Gholam Hossein; Tiekink, Edward R. T.; Mirtamizdoust, Babak
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2011
• Journal volume: 67
• Journal issue: 12
• Pages of publication: m1729 - m1730
• a: 11.2122 ± 0.0014 Å
• b: 13.4644 ± 0.0017 Å
• c: 14.1451 ± 0.0018 Å
• α: 90°
• β: 111.906 ± 0.002°
• γ: 90°
• Cell volume: 1981.2 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0378
• Residual factor for significantly intense reflections: 0.0237
• Weighted residual factors for significantly intense reflections: 0.0591
• Weighted residual factors for all reflections included in the refinement: 0.0656
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes