Information card for entry 4035683

Structure parameters

• Formula: C27 H47 N O5 S Si
• Calculated formula: C27 H47 N O5 S Si
• Title of publication: Acyclic Remote 1,5- and 1,4,5-Stereocontrol in the Catalytic Stereoselective Reactions of β-Lactams with Aldehydes: The Effect of the N-Methylimidazole Ligand.
• Authors of publication: Plata, Paulina; Klimczak, Urszula; Zambroń, Bartosz K
• Journal of publication: The Journal of organic chemistry
• Year of publication: 2018
• Journal volume: 83
• Journal issue: 23
• Pages of publication: 14527 - 14552
• a: 11.2358 ± 0.0004 Å
• b: 12.6433 ± 0.0004 Å
• c: 22.2439 ± 0.0007 Å
• α: 103.677 ± 0.002°
• β: 95.436 ± 0.002°
• γ: 97.749 ± 0.002°
• Cell volume: 3015.85 ± 0.18 ų
• Cell temperature: 164 ± 2 K
• Ambient diffraction temperature: 164 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1635
• Residual factor for significantly intense reflections: 0.0602
• Weighted residual factors for significantly intense reflections: 0.133
• Weighted residual factors for all reflections included in the refinement: 0.1579
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No