Solvent-Controlled, Site-Selective N-Alkylation Reactions of Azolo-Fused Ring Heterocycles at N1-, N2-, and N3-Positions, Including Pyrazolo[3,4- d]pyrimidines, Purines, [1,2,3]Triazolo[4,5]pyridines, and Related Deaza-Compounds.
Authors of publication
Bookser, Brett C.; Weinhouse, Michael I.; Burns, Aaron C.; Valiere, Andrew N.; Valdez, Lino J.; Stanczak, Pawel; Na, Jim; Rheingold, Arnold L.; Moore, Curtis E.; Dyck, Brian
Journal of publication
The Journal of organic chemistry
Year of publication
2018
Journal volume
83
Journal issue
12
Pages of publication
6334 - 6353
a
8.095 ± 0.013 Å
b
13.644 ± 0.014 Å
c
7.107 ± 0.008 Å
α
90°
β
114.09 ± 0.04°
γ
90°
Cell volume
716.6 ± 1.6 Å3
Cell temperature
100 K
Ambient diffraction temperature
100 K
Number of distinct elements
4
Space group number
9
Hermann-Mauguin space group symbol
C 1 c 1
Hall space group symbol
C -2yc
Residual factor for all reflections
0.0335
Residual factor for significantly intense reflections
0.0314
Weighted residual factors for significantly intense reflections
0.0734
Weighted residual factors for all reflections included in the refinement
0.0743
Goodness-of-fit parameter for all reflections included in the refinement
