Solvent-Controlled, Site-Selective N-Alkylation Reactions of Azolo-Fused Ring Heterocycles at N1-, N2-, and N3-Positions, Including Pyrazolo[3,4- d]pyrimidines, Purines, [1,2,3]Triazolo[4,5]pyridines, and Related Deaza-Compounds.
Authors of publication
Bookser, Brett C.; Weinhouse, Michael I.; Burns, Aaron C.; Valiere, Andrew N.; Valdez, Lino J.; Stanczak, Pawel; Na, Jim; Rheingold, Arnold L.; Moore, Curtis E.; Dyck, Brian
Journal of publication
The Journal of organic chemistry
Year of publication
2018
Journal volume
83
Journal issue
12
Pages of publication
6334 - 6353
a
3.8226 ± 0.0005 Å
b
7.1075 ± 0.0012 Å
c
27.806 ± 0.004 Å
α
90°
β
90°
γ
90°
Cell volume
755.46 ± 0.19 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 K
Number of distinct elements
4
Space group number
19
Hermann-Mauguin space group symbol
P 21 21 21
Hall space group symbol
P 2ac 2ab
Residual factor for all reflections
0.043
Residual factor for significantly intense reflections
0.0403
Weighted residual factors for significantly intense reflections
0.1067
Weighted residual factors for all reflections included in the refinement
0.1089
Goodness-of-fit parameter for all reflections included in the refinement
