Total Syntheses of the 3H-Pyrrolo[2,3-c]quinolone-containing Alkaloids Marinoquinolines A-F, K and Aplidiopsamine A Using a Palladium-catalysed Ullmann Cross-coupling/Reductive Cyclization Pathway.
Authors of publication
Bolte, Benoit; Bryan, Christopher S.; Sharp, Phillip P.; Sayyahi, Soheil; Rihouey, Charly; Kendrick, Amy; Lan, Ping; Banwell, Martin G.; Jackson, Colin J.; Fraser, Nicholas J.; Willis, Anthony C.; Ward, James S.
Journal of publication
The Journal of organic chemistry
Year of publication
2019
a
14.0236 ± 0.0002 Å
b
15.8376 ± 0.0002 Å
c
19.3464 ± 0.0002 Å
α
90°
β
107.46 ± 0.0007°
γ
90°
Cell volume
4098.88 ± 0.09 Å3
Cell temperature
200 K
Ambient diffraction temperature
200 K
Number of distinct elements
3
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0519
Residual factor for significantly intense reflections
0.0381
Weighted residual factors for all reflections
0.096
Weighted residual factors for significantly intense reflections
0.0883
Weighted residual factors for all reflections included in the refinement
0.096
Goodness-of-fit parameter for all reflections included in the refinement
