Total Syntheses of the 3H-Pyrrolo[2,3-c]quinolone-containing Alkaloids Marinoquinolines A-F, K and Aplidiopsamine A Using a Palladium-catalysed Ullmann Cross-coupling/Reductive Cyclization Pathway.
Authors of publication
Bolte, Benoit; Bryan, Christopher S.; Sharp, Phillip P.; Sayyahi, Soheil; Rihouey, Charly; Kendrick, Amy; Lan, Ping; Banwell, Martin G.; Jackson, Colin J.; Fraser, Nicholas J.; Willis, Anthony C.; Ward, James S.
Journal of publication
The Journal of organic chemistry
Year of publication
2019
a
17.2396 ± 0.0002 Å
b
17.2396 ± 0.0002 Å
c
8.5097 ± 0.0002 Å
α
90°
β
90°
γ
90°
Cell volume
2529.12 ± 0.07 Å3
Cell temperature
200 K
Ambient diffraction temperature
200 K
Number of distinct elements
3
Space group number
114
Hermann-Mauguin space group symbol
P -4 21 c
Hall space group symbol
P -4 2n
Residual factor for all reflections
0.0367
Residual factor for significantly intense reflections
0.033
Weighted residual factors for all reflections
0.0843
Weighted residual factors for significantly intense reflections
0.0815
Weighted residual factors for all reflections included in the refinement
0.0843
Goodness-of-fit parameter for all reflections included in the refinement
