Total Syntheses of the 3H-Pyrrolo[2,3-c]quinolone-containing Alkaloids Marinoquinolines A-F, K and Aplidiopsamine A Using a Palladium-catalysed Ullmann Cross-coupling/Reductive Cyclization Pathway.
Authors of publication
Bolte, Benoit; Bryan, Christopher S.; Sharp, Phillip P.; Sayyahi, Soheil; Rihouey, Charly; Kendrick, Amy; Lan, Ping; Banwell, Martin G.; Jackson, Colin J.; Fraser, Nicholas J.; Willis, Anthony C.; Ward, James S.
Journal of publication
The Journal of organic chemistry
Year of publication
2019
a
5.845 ± 0.0001 Å
b
10.0578 ± 0.0002 Å
c
14.217 ± 0.0003 Å
α
90°
β
90°
γ
90°
Cell volume
835.79 ± 0.03 Å3
Cell temperature
150 K
Ambient diffraction temperature
150 K
Number of distinct elements
3
Space group number
19
Hermann-Mauguin space group symbol
P 21 21 21
Hall space group symbol
P 2ac 2ab
Residual factor for all reflections
0.061
Residual factor for significantly intense reflections
0.0428
Weighted residual factors for all reflections
0.0909
Weighted residual factors for significantly intense reflections
0.0803
Weighted residual factors for all reflections included in the refinement
0.0909
Goodness-of-fit parameter for all reflections included in the refinement
