Total Syntheses of the 3H-Pyrrolo[2,3-c]quinolone-containing Alkaloids Marinoquinolines A-F, K and Aplidiopsamine A Using a Palladium-catalysed Ullmann Cross-coupling/Reductive Cyclization Pathway.
Authors of publication
Bolte, Benoit; Bryan, Christopher S.; Sharp, Phillip P.; Sayyahi, Soheil; Rihouey, Charly; Kendrick, Amy; Lan, Ping; Banwell, Martin G.; Jackson, Colin J.; Fraser, Nicholas J.; Willis, Anthony C.; Ward, James S.
Journal of publication
The Journal of organic chemistry
Year of publication
2019
a
16.1616 ± 0.0006 Å
b
9.5535 ± 0.0003 Å
c
18.608 ± 0.0006 Å
α
90°
β
90°
γ
90°
Cell volume
2873.07 ± 0.17 Å3
Cell temperature
200 K
Ambient diffraction temperature
200 K
Number of distinct elements
3
Space group number
61
Hermann-Mauguin space group symbol
P b c a
Hall space group symbol
-P 2ac 2ab
Residual factor for all reflections
0.0745
Residual factor for significantly intense reflections
0.0457
Weighted residual factors for all reflections
0.1187
Weighted residual factors for significantly intense reflections
0.1017
Weighted residual factors for all reflections included in the refinement
0.1187
Goodness-of-fit parameter for all reflections included in the refinement
