Information card for entry 4038867
| Formula |
C42 H58 N2 P4 |
| Calculated formula |
C42 H58 N2 P4 |
| Title of publication |
Dynamic covalent chemistry approach toward 18-membered P<sub>4</sub>N<sub>2</sub> macrocycles and their nickel(II) complexes. |
| Authors of publication |
Musina, Elvira I.; Wittmann, Tatiana I.; Musin, Lenar; Balueva, Anna S.; Shpagina, Alena S.; Litvinov, Igor A.; Lönnecke, Peter; Hey-Hawkins, Evamarie; Karasik, Andrey A.; Sinyashin, Oleg G. |
| Journal of publication |
The Journal of organic chemistry |
| Year of publication |
2020 |
| a |
21.8967 ± 0.0007 Å |
| b |
8.026 ± 0.0002 Å |
| c |
25.7249 ± 0.0011 Å |
| α |
90° |
| β |
111.928 ± 0.004° |
| γ |
90° |
| Cell volume |
4193.9 ± 0.3 Å3 |
| Cell temperature |
130 ± 2 K |
| Ambient diffraction temperature |
130 ± 2 K |
| Number of distinct elements |
4 |
| Space group number |
15 |
| Hermann-Mauguin space group symbol |
C 1 2/c 1 |
| Hall space group symbol |
-C 2yc |
| Residual factor for all reflections |
0.061 |
| Residual factor for significantly intense reflections |
0.043 |
| Weighted residual factors for significantly intense reflections |
0.093 |
| Weighted residual factors for all reflections included in the refinement |
0.101 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.028 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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https://www.crystallography.net/4038867.html
