Information card for entry 4038868
| Formula |
C48 H66 N2 P4 |
| Calculated formula |
C48 H66 N2 P4 |
| Title of publication |
Dynamic covalent chemistry approach toward 18-membered P<sub>4</sub>N<sub>2</sub> macrocycles and their nickel(II) complexes. |
| Authors of publication |
Musina, Elvira I.; Wittmann, Tatiana I.; Musin, Lenar; Balueva, Anna S.; Shpagina, Alena S.; Litvinov, Igor A.; Lönnecke, Peter; Hey-Hawkins, Evamarie; Karasik, Andrey A.; Sinyashin, Oleg G. |
| Journal of publication |
The Journal of organic chemistry |
| Year of publication |
2020 |
| a |
12.6527 ± 0.0007 Å |
| b |
13.775 ± 0.0007 Å |
| c |
16.0646 ± 0.0005 Å |
| α |
104.584 ± 0.004° |
| β |
98.638 ± 0.003° |
| γ |
115.784 ± 0.005° |
| Cell volume |
2329 ± 0.2 Å3 |
| Cell temperature |
130 ± 2 K |
| Ambient diffraction temperature |
130 ± 2 K |
| Number of distinct elements |
4 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.1245 |
| Residual factor for significantly intense reflections |
0.0601 |
| Weighted residual factors for significantly intense reflections |
0.0995 |
| Weighted residual factors for all reflections included in the refinement |
0.1246 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.008 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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https://www.crystallography.net/4038868.html
