Information card for entry 4038870
| Chemical name |
1,10-Di(4?-methylbenzyl)-3,8,12,17-(RSSR)-tetra(pyridine-2?-yl)-3,8,12,17- tetraoxo-1,10-diaza?3,8,12,17?tetraphosphacyclooctadecane |
| Formula |
C24 H29 N3 O2 P2 |
| Calculated formula |
C24 H29 N3 O2 P2 |
| Title of publication |
Dynamic covalent chemistry approach toward 18-membered P<sub>4</sub>N<sub>2</sub> macrocycles and their nickel(II) complexes. |
| Authors of publication |
Musina, Elvira I.; Wittmann, Tatiana I.; Musin, Lenar; Balueva, Anna S.; Shpagina, Alena S.; Litvinov, Igor A.; Lönnecke, Peter; Hey-Hawkins, Evamarie; Karasik, Andrey A.; Sinyashin, Oleg G. |
| Journal of publication |
The Journal of organic chemistry |
| Year of publication |
2020 |
| a |
10.11 ± 0.03 Å |
| b |
11.896 ± 0.016 Å |
| c |
12.699 ± 0.017 Å |
| α |
113.23 ± 0.016° |
| β |
104.32 ± 0.02° |
| γ |
98.18 ± 0.02° |
| Cell volume |
1310 ± 5 Å3 |
| Cell temperature |
296 ± 2 K |
| Ambient diffraction temperature |
296 ± 2 K |
| Number of distinct elements |
5 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.2882 |
| Residual factor for significantly intense reflections |
0.0788 |
| Weighted residual factors for significantly intense reflections |
0.1697 |
| Weighted residual factors for all reflections included in the refinement |
0.2549 |
| Goodness-of-fit parameter for all reflections included in the refinement |
0.891 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/4038870.html
