Information card for entry 4063191

Structure parameters

• Formula: C32 H41 Os P Si
• Calculated formula: C32 H20 Os P Si
• SMILES: [OsH2]12345([P](C(C)C)(C(C)C)C(C)C)[c]6([Si](c7c5cccc7)(c5ccccc5)c5ccccc5)[cH]1[cH]2[cH]3[cH]46
• Title of publication: Generation of Functionally Substituted Cyclopentadienyl Ligands in Osmium(IV) Chemistry
• Authors of publication: Miguel Baya; Pascale Crochet; Miguel A. Esteruelas; Enrique Oñate
• Journal of publication: Organometallics
• Year of publication: 2001
• Journal volume: 20
• Pages of publication: 240 - 253
• a: 10.677 ± 0.001 Å
• b: 11.171 ± 0.002 Å
• c: 13.241 ± 0.002 Å
• α: 85.53 ± 0.01°
• β: 72.32 ± 0.01°
• γ: 80.04 ± 0.01°
• Cell volume: 1481.5 ± 0.4 ų
• Cell temperature: 200 ± 0.2 K
• Ambient diffraction temperature: 200 ± 0.2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0499
• Residual factor for significantly intense reflections: 0.0439
• Weighted residual factors for significantly intense reflections: 0.1181
• Weighted residual factors for all reflections included in the refinement: 0.124
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No