Information card for entry 4063192

Structure parameters

• Formula: C38 H52 Ge N Os P
• Calculated formula: C38 H52 Ge N Os P
• SMILES: [OsH2]1234([Ge](c5ccccc5)(c5ccccc5)c5ccccc5)([P](C(C)C)(C(C)C)C(C)C)[c]5([cH]1[cH]2[cH]3[cH]45)N(CC=C)CC=C
• Title of publication: Generation of Functionally Substituted Cyclopentadienyl Ligands in Osmium(IV) Chemistry
• Authors of publication: Miguel Baya; Pascale Crochet; Miguel A. Esteruelas; Enrique Oñate
• Journal of publication: Organometallics
• Year of publication: 2001
• Journal volume: 20
• Pages of publication: 240 - 253
• a: 12.345 ± 0.002 Å
• b: 20.975 ± 0.002 Å
• c: 13.932 ± 0.002 Å
• α: 90°
• β: 91.07 ± 0.02°
• γ: 90°
• Cell volume: 3606.9 ± 0.9 ų
• Cell temperature: 298 ± 0.2 K
• Ambient diffraction temperature: 298 ± 0.2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0455
• Residual factor for significantly intense reflections: 0.0317
• Weighted residual factors for significantly intense reflections: 0.0792
• Weighted residual factors for all reflections included in the refinement: 0.0875
• Goodness-of-fit parameter for all reflections included in the refinement: 0.994
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No