Group 1 Bis(iminophosphorano)methanides, Part 1:N-Alkyl and Silyl Derivatives of the Sterically Demanding Methanes H2C(PPh2NR)2(R = Adamantyl and Trimethylsilyl)
Authors of publication
Wooles, Ashley J.; Gregson, Matthew; Cooper, Oliver J.; Middleton-Gear, Amy; Mills, David P.; Lewis, William; Blake, Alexander J.; Liddle, Stephen T.
Journal of publication
Organometallics
Year of publication
2011
Journal volume
30
Journal issue
20
Pages of publication
5314
a
13.8885 ± 0.0002 Å
b
16.7771 ± 0.0004 Å
c
38.3042 ± 0.0005 Å
α
90°
β
96.1663 ± 0.0013°
γ
90°
Cell volume
8873.6 ± 0.3 Å3
Cell temperature
90 ± 2 K
Ambient diffraction temperature
90 ± 2 K
Number of distinct elements
7
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0532
Residual factor for significantly intense reflections
0.0484
Weighted residual factors for significantly intense reflections
0.1231
Weighted residual factors for all reflections included in the refinement
0.1261
Goodness-of-fit parameter for all reflections included in the refinement
