Information card for entry 4066350

Structure parameters

• Formula: C22 H43 Rh Si3
• Calculated formula: C22 H43 Rh Si3
• SMILES: [Rh]123456([c]7([c]4([c]3([c]2([c]17C)C)C)C)[Si](C)(C)C)(C=[CH]5[Si](C)(C)C)C=[CH]6[Si](C)(C)C
• Title of publication: Synthesis of Rhodium Complexes with Bulky Substituted Cyclopentadienyl Ligands. H/D Exchange Reactions and Silane Activation†
• Authors of publication: Esqueda, Ana Cristina; Conejero, Salvador; Maya, Celia; Carmona, Ernesto
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 21
• Pages of publication: 5481
• a: 9.8836 ± 0.0002 Å
• b: 13.5588 ± 0.0003 Å
• c: 19.9952 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2679.55 ± 0.1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0285
• Residual factor for significantly intense reflections: 0.0254
• Weighted residual factors for significantly intense reflections: 0.0635
• Weighted residual factors for all reflections included in the refinement: 0.0647
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No