Information card for entry 4067856

Structure parameters

• Formula: C31 H59 P2 S2 Si4 Sn
• Calculated formula: C31 H59 P2 S2 Si4 Sn
• Title of publication: Hypervalent Sulfur-Functionalized Diphosphagermylene and Diphosphastannylene Compounds
• Authors of publication: Izod, Keith; Clark, Ewan R.; Clegg, William; Harrington, Ross W.
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 1
• Pages of publication: 246
• a: 10.4746 ± 0.0002 Å
• b: 21.3062 ± 0.0004 Å
• c: 18.4807 ± 0.0003 Å
• α: 90°
• β: 102.312 ± 0.0019°
• γ: 90°
• Cell volume: 4029.56 ± 0.13 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0387
• Residual factor for significantly intense reflections: 0.023
• Weighted residual factors for significantly intense reflections: 0.0478
• Weighted residual factors for all reflections included in the refinement: 0.0495
• Goodness-of-fit parameter for all reflections included in the refinement: 0.902
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No